User Tools

Site Tools


vapor_silanation_rig_sop

Differences

This shows you the differences between two versions of the page.

Link to this comparison view

Both sides previous revisionPrevious revision
Next revision
Previous revision
vapor_silanation_rig_sop [2022/08/26 22:36] – [Operating Guidelines] haleyvapor_silanation_rig_sop [2023/04/04 21:28] (current) – [References] haley
Line 1: Line 1:
-====== Vapor Silanation Rig Safe Operating Procedures ======+====== Vapor Silanization Rig Safe Operating Procedures ====== 
 +4/4/23 Haley Holcomb haleyholcomb@ucsb.edu
 ===== Location ===== ===== Location =====
-The vapor silanation rig is located in the first fume hood you see to your left when you walk in the door+The vapor silanization rig is located in the first fume hood you see to your left when you walk in the door
 of the microfluidics lab, Elings 3430. of the microfluidics lab, Elings 3430.
 ===== Safety ===== ===== Safety =====
 Trimethylchlorosilane is flammable, toxic, and reacts with water vapor. It can make you sick if inhaled Trimethylchlorosilane is flammable, toxic, and reacts with water vapor. It can make you sick if inhaled
-and ignite if it reacts with air or water vapor. It may only be used in the vapor silination rig inside of a fume hood. Do not let the pressure inside the chamber exceed 15 in Hg. The silane valve must always+and ignite if it reacts with air or water vapor. It may only be used in the vapor silanization rig inside of a fume hood. Do not let the pressure inside the chamber exceed 15 in Hg. The silane valve must always
 be opened in a nitrogen atmosphere. Protective eyewear, a lab coat, and gloves must be worn. Make be opened in a nitrogen atmosphere. Protective eyewear, a lab coat, and gloves must be worn. Make
 sure the fume hood is closed when you are not working inside of it. Do not handle the silane without sure the fume hood is closed when you are not working inside of it. Do not handle the silane without
Line 31: Line 32:
   - Close the fume hood and set a timer for 40 minutes.   - Close the fume hood and set a timer for 40 minutes.
   - Update the logbook with your end time.   - Update the logbook with your end time.
-  - When your timer goes off, open the nitrogen valve until the pressure reads 5 in Hg. Open the vacuum valve until 15 in Hg. Repeat 5 times to purge the chamber again+  - When your timer goes off, close the silane valves (perpendicular). 
-  - Close the silane valves (perpendicular).+  - Open the nitrogen valve until the pressure reads 5 in Hg. Open the vacuum valve until 15 in Hg. Repeat 5 times to purge the chamber again.
   - Remove your wafer.   - Remove your wafer.
   - Flip the sign back to “AVAILABLE” and close the hood.   - Flip the sign back to “AVAILABLE” and close the hood.
 ===== References ===== ===== References =====
-{{ :changing_silane_container_sop.pdf |}} +  * {{ :changing_silane_container_sop.pdf |}} 
-{{ :tools:vaporsilanationrig:tmcs_msds.pdf |}} +  {{ :tools:vaporsilanationrig:tmcs_msds.pdf |}} 
-{{ :vapor_silanation_rig_sop_2_.pdf |}}+  {{ :vapor_silanization_rig_sop.pdf |}} 
  
vapor_silanation_rig_sop.1661553410.txt.gz · Last modified: 2022/08/26 22:36 by haley